Distillation - Part 1: Essential Oils

in #food8 years ago

Greetings, 

In this article I will demonstrate how essential oils are distilled from plants.  

Distillation involves heating a liquid, condensing the steam back into liquid form and collecting the distillate in a vessel.    

Types of Stills

Copper Alembic Still   

Copper stills are by far the most beautiful and expensive stills available. This photo is of my first still which was handmade in France. 

This particular model’s capacity is 1.5 liters (0.7 gallons) which makes it impractical for distilling large quantities of essential oil. These pups run for around 150 steem dollars.    

Steam Injection 

(image source)

This is a common laboratory distillation setup. 

The flask on the bottom is filled with water and heated which injects steam through the chopped plant material in the upper flask.  The steam, which is now carrying the water soluble components and volatile oils, condenses as it passes through the water cooled condenser coil. 

A glass essencier attachment separates the oil from the hydrosol (water solution).   

Labware is easy to customize and replacing broken parts is simple. It is also transparent. The only downside is that most labware setups have somewhat small chambers so are not useful for distilling large quantities of herbs.   

Modified Pressure Cooker   

To extract larger batches of herbs, I simply attached a tube to the top of a pressure cooker and attached the tube to my copper condenser coil. 

With a little ingenuity and some basic supplies, a still can easily be made at home. 

Here is a simple design I’ve drawn up which should give you the general idea of what’s required:   

Moonshine Still   

I spent long hours searching the perfect still and decided on this one from Brewhaus. It is useful for both distilling essential oils and making alcohol. 

Finely crafted from high grade stainless steel, this still has an 8-gallon capacity and includes everything needed to start distilling. The quality of craftsmanship and simplicity of design is well worth the 17 ounces of silver paid. 


Distillation of Helichrysum                

Helichrysum (helichrysum italicum) also known as "Imortelle" is a highly aromatic herb that is used in perfumery, skin care products and as a medicine. It has a high essential oil content, as with other aromatic herbs. 

I harvested the flowering plant this morning, a time when the essential oil content is the highest. Throughout the day, the essential oils in plants dissipate and are replenished overnight.

The herb is chopped, placed in the pot of the still and covered with water. Chopping the herb opens up the cell walls and makes extracting the oil more efficient.

All the tubes are connected, the heat is on and distillation commences. 

The condenser on this model consists of a pipe that the distillate travels through, surrounded by another pipe filled with cold water. Water is cycled through the two clear plastic tubes and the distillate travels down the opaque tube into a collection vessel.

The distillate is collected in a separatory funnel which is a glass vessel with a valve at the bottom. The essential oil rises to the surface of the hydrosol. The hydrosol is drained every so often and the essential oil is left behind.

After a few hours of distilling, the process is complete. The hyrdosol is completely drained, then the oil is drained into a glass dropper bottle.


The yield from this plant was very good. This summer I've distilled nettles, mint, male cannabis plants and cedar leaf which all had considerable yields.  


Other ways of separating the oil from the hydrosol include:

  • Freezing. The hyrdosol freezes and the oil is left in liquid form then poured or siphoned off the top.
  • Essencier. With this attachment, the oil and hyrdol are automatically separated throughout the distillation process.
  • Siphoning. The oil is siphoned from the top of the hydrosol.


The Laboratory

My laboratory is inside of a trailer that has been converted into a commercial kitchen. It is a clean, dedicated space for doing herbal extractions.


I hope you enjoyed reading this article and learning about essential oils. In due time I will share how to make your own "rubbing alcohol".



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Nice pictures. Reminds me a bit of the most expensive cup of coffee I ever ordered:

Probably not worth £7, but fun.

That is really cool. Who knows, it might come in handy one day.

can you use one of those set-ups or cannabis?

There are a lot of conflicting stories on whether or not you can steam distill cannabis. I'm not sure on the best way yet but recently distilled some dried cannabis flowers from last year. The yield was good but most of the oil/resin stuck to the side of the collection vessel. I poured out the hydrosol and dissolved the oil/resin with alcohol, let the alcohol evaporate and was left with a nice, green oil. I tasted the tiniest amount possible and it got me ripped!

Slingshot is a Netflix documentary that tells the story about Dean Kamen's invention that turns any water into clean drinking water. It has the potential to save the world from a massive water crisis. Highly recommended.

Distillation is the purest form of water. Despite this, those planning on becoming wealthy from the water shortage will try to derail it.

Thank you vegascomic, I will check it out. The slingshot invention certainly steps up the distillation process.

Distilled water may become one of the major sources of clean drinking water in the not far future. Derail it or profit from it. There will be those with stills, those with bottled water and some with bamboo filtration tubes filled with sand and moss.

Awesome post and lab setup! I checked out some of your other posts as well and must say I'm impressed by your garden, especially your cacti. ;) Gotta love the smell of Helichrysum, too. Upvoted!

Thank you, I'm happy that you enjoy what I have to share. You're posts are interesting to me as well, I'm a follower :)

Likewise, and looking forward to your future posts!

Nice, this could be a little money making venture indoors.

Hi there....I sell labware....I want to sell it online with steem......i can sell big trademarks but also more economic products(low cost) from Chinese manufacturers lol...if you use it I can make you at price of cost in exchange for resteems ahah...all the best

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